液相色谱—串联质谱法测定木材及木制品中3种异噻唑啉酮类防腐剂
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1.山东临沂出入境检验检疫局 临沂 276034;2.山东出入境检验检疫局 青岛 266001

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山东出入境检验检疫局科技项目“液相色谱-串联质谱法(LC-MS/MS)检测饲料中异噻唑啉酮类防腐剂方法研究”(SK201460)。


Determination of Three Isothiazolinong Preservatives in wood and wood Products Using Liquid Chromatography Tandem Mass Spectrometry
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1.Shangdong Linyi Entry Inspection and Quarantine Bureau Linyi 276034;2.Shangdong Entry Inspection and Quarantine Bureau Qingdao 266001

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    摘要:

    摘要:本文建立了一种木材及木制品中3种异噻唑啉酮类防腐剂的检测方法,采用超声法甲醇提取,离心后浓缩定容,利用液相色谱-串联质谱法进行检测。该方法操作简单,准确度高,回收率在85%~111%,相对标准偏差为0.93%~8.20%,提取效果较好。

    Abstract:

    Abstract:A method for determination of three isothiazolinone preservatives in wood and wood products was developed.We extracted the preservatives from the samples by ultrasonic extraction with methanol,and centrifuged the extract and diluted the concentrate,and then determined by liquid chromatography tandem mass spectrometry.The method was easily to handle and had a preferable extracting effect.The recovery rate was distributed in the range of 85%~111% and the relative standard deviation was distributed from 0.93% to 8.20%.

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.液相色谱—串联质谱法测定木材及木制品中3种异噻唑啉酮类防腐剂[J].湖北林业科技,2016,(3):

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  • 在线发布日期: 2016-10-09
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